Diisobutylamine → HCID 18948397, compound

HRID 1768604Notes

Reaction equation

[CH2:1]([NH:5][CH2:6][CH:7]([CH3:9])[CH3:8])[CH:2]([CH3:4])[CH3:3].Br[CH2:11][C:12]([O:14][CH3:15])=[O:13]>>[CH2:1]([N:5]([CH2:6][CH:7]([CH3:9])[CH3:8])[CH2:11][C:12]([O:14][CH3:15])=[O:13])[CH:2]([CH3:4])[CH3:3]

Participants

Reactant 2

HCID 8085Diisobutylamine

HCID 60984Methyl bromoacetate

Product 1

HCID 18948397HCID 18948397, compound

Procedure

Following a procedure similar to that described in Preparation 47(a) 5.17 g (40 mmole) of N,N-diisobutylamine and 3.06 g (20 mmole) of methyl bromoacetate were reacted together, to give 4.02 g of the title compound as a white powder.

Workup

customwere reacted together

Sources & evidence

ORD record: ord-24b6cfdf78fe46f6aa06f9a3064ccdfe
Source dataset: uspto-grants-1995_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05378690

Reaction notes

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