HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxybenzaldehyde → Benzaldehyde, 3-(2-hydroxyethoxy)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxybenzaldehyde | HCID 101 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Ethanol, 1-bromo- | HCID 14202443 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Benzaldehyde, 3-(2-hydroxyethoxy)- | HCID 6453965 | — |
Reaction Steps
1.42 g of sodium were dissolved in 200 ml of ethanol. 7.5 g of 3-hydroxybenzaldehyde and 10.5 g of bromoethanol were added and the resulting solution was refluxed for 5 hours. The solution was purified by column chromatography (silica, CH2Cl2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05378718 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-c45f1b75c2e1437fa0065d8d13b3d929 |
| Source note | uspto-grants-1995_01 |