HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylaldehyde → HCID 18948998, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylaldehyde | HCID 6998 | — |
| Reactant | 2-(2-(2-Chloroethoxy)ethoxy)ethanol | HCID 78871 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18948998 | HCID 18948998 | — |
Reaction Steps
A solution of 10 g of sodium salt of salicylaldehyde and 10 g of 2-[2-(2-chloroethoxy)ethoxy]ethanol in dimethylformamide was refluxed for 50 hours. After evaporation, the residue was dissolved in ethyl acetate and the solution washed with water, dried over magnesium sulfate and evaporated. The compound was purified by chromatography (silica; ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05378718 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-1640a345deb34f44aeb9c1c33ceb028c |
| Source note | uspto-grants-1995_01 |