Hydroxylamine → HCID 14860691, compound

Participants

Reaction Steps

Using ethyl 2-bromo-2-acetamidoacetate (2.10 g, 9.37 mmol) and anhydrous NH2OH (0.93 g, 28.00 mmol) gave an oily residue. The residue was purified by flash column chromatography on SiO2 gel (5% MeOH/CHCl3) to give the desired product. The product was recrystallized from EtOH to give a white flaky solid.

Provenance & Evidence