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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1768897Generated: November 1, 2026

Azobisisobutyronitrile → Butyl 2-methylprop-2-enoate--ethenylbenzene (1/1)

https://huagongshe.com/reaction/1768897

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAzobisisobutyronitrileHCID 6547—
ReactantButyl MethacrylateHCID 7354—
ReactantStyreneHCID 7501—
ProductButyl 2-methylprop-2-enoate--ethenylbenzene (1/1)HCID 160004—

Reaction Conditions

Temperature110 °C

Reaction Steps

With the addition of 2,2'-azobisisobutyronitrile, a mixture of styrene and n-butyl methacrylate at a mixing ratio of (75:25) was stirred at temperatures of 100 to 120° C. in order to obtain 43 parts by weight of a styrene-n-butyl methacrylate copolymer. The previously obtained solution was further added dropwise to the above polymerization mixture and the polymerization was allowed to continue for three hours. Thereafter, a solvent component was removed from the above mixture by heating under vacuum.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05380616
Source datasetuspto-grants-1995_01
ORD IDord-ab30ceebb68f49f4b5f0e5904e754478
Source noteuspto-grants-1995_01