HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → HCID 18946530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 18946541 | HCID 18946541 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18946530 | HCID 18946530 | — |
Reaction Steps
The above alcohol (0.6 g) was oxidised under Swern conditions (dimethyl sulphoxide (0.26 g) oxalyl chloride (160 μl), triethylamine (1.0 ml)) in dichloromethane (30 ml) to give 8-(3,5-bistrifluoromethyl-2-pyridyloxy)octan-1-al. This was used directly in the next stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05380732 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-821eb56333a94ad881fc0ad072cf7604 |
| Source note | uspto-grants-1995_01 |