HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium hexafluorophosphate → HCID 86748381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium hexafluorophosphate | HCID 23688904 | — |
| Reactant | HCID 86748380 | HCID 86748380 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86748381 | HCID 86748381 | 66.4% |
Reaction Steps
1-(p-methoxybenzyl)pyridine-2-carboxaldehyde ethylene acetal chloride (10.0 g) was dissolved in water (100 mL) and was treated with potassium hexafluorophosphate (10.0 g). The precipitate which formed was collected by filtration and dried at 60° C. in vacuo to afford 9 g of 1-(p-methoxybenzyl)pyridine-2-carboxaldehyde ethylene acetal hexafluorophosphate (Formula X: R1 =R7 =H; R2 =4'--OCH3 ; X- =PF6-).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05380729 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-724decd9d8b64c259ca69f44c96966b1 |
| Source note | uspto-grants-1995_01 |