HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 18946568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 19023639 | HCID 19023639 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18946568 | HCID 18946568 | — |
Reaction Steps
By carrying out the procedure according to Example 10 which is described above, the compound 2-[(1-acetyl-2-indolyl ) carbonylamino]-4-phenyl-5-ethoxycarbonylthiazole (1.5 g) is prepared and dissolved in 100 ml of ethanol in the presence of 0.6 g of Na2CO3. The mixture is stirred at room temperature for 48 hours and then concentrated under vacuum. The residue is triturated in water and then in a minimum amount of dichloromethane, filtered and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05380736 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-41139a09542f4bcd86e39e113572b181 |
| Source note | uspto-grants-1995_01 |