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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1769438Generated: October 31, 2026

HCID 53809102, compound → HCID 53721009, compound

https://huagongshe.com/reaction/1769438

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 53809102HCID 53809102—
ReactantHCID 178418361HCID 178418361—
SolventEthanolHCID 702—
ProductHCID 53721009HCID 5372100998.7%

Reaction Steps

To a solution of 445 mg of N-(1-diethoxyphosphoryl-3-phenylpropyl)-leucine benzyl ester in 10 ml of ethanol was added 100 mg of 10% Pd--C, after which the mixture was stirred vigorously under atmospheric pressure of hydrogen at room temperature for 24 hours. The Pd--C was filtered off, and the solvent was distilled off to yield the title compound as a light-yellow oil (356 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05380921
Source datasetuspto-grants-1995_01
ORD IDord-1b5d33d243804e2a9111eaabb6338794
Source noteuspto-grants-1995_01