HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53809102, compound → HCID 53721009, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53809102 | HCID 53809102 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53721009 | HCID 53721009 | 98.7% |
Reaction Steps
To a solution of 445 mg of N-(1-diethoxyphosphoryl-3-phenylpropyl)-leucine benzyl ester in 10 ml of ethanol was added 100 mg of 10% Pd--C, after which the mixture was stirred vigorously under atmospheric pressure of hydrogen at room temperature for 24 hours. The Pd--C was filtered off, and the solvent was distilled off to yield the title compound as a light-yellow oil (356 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05380921 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-1b5d33d243804e2a9111eaabb6338794 |
| Source note | uspto-grants-1995_01 |