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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1769576Generated: November 1, 2026

HCID 57052782, compound → HCID 86748402, compound

https://huagongshe.com/reaction/1769576

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57052782HCID 57052782—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 86748402HCID 8674840290.2%

Reaction Steps

1,1-Ethylenedioxy-4-(3',5'-difluoro-4'-trifluoromethylphenyl)-3-cyclohexene (17.3 g) was dissolved in ethanol (200 ml), followed by adding Pd/C (5%) (5 g), carrying out a catalytic reduction with stirring in a hydrogen gas atmosphere, filtering off the catalyst after completion of the reaction, and distilling off the organic layer under reduced pressure, to obtain 1,1-ethylenedioxy-4-(3',5'-difluoro-4'-trifluoromethylphenyl)cyclohexane (15.7 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05382379
Source datasetuspto-grants-1995_01
ORD IDord-05886c0c298b4ffdaea151de4e3c0915
Source noteuspto-grants-1995_01