HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54188169, compound → HCID 54100496, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54188169 | HCID 54188169 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54100496 | HCID 54100496 | 97.8% |
Reaction Steps
4-(2'-(3",4",5"-Trifluorophenyl)ethenyl)cyclohexanone (71 g) was dissolved in ethanol (500 ml), followed by adding Pd/C (5%) (2.0 g), hydrogenating the compound in a hydrogen gas atmosphere with stirring till the hydrogen absorption was completed, filtering off the catalyst after completion of the reaction, and concentrating the solvent under reduced pressure, to obtain 4-(2'-(3",4",5"-trifluorophenyl)ethyl)cyclohexanone (70 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05382379 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-16b7281a90f04087b884076e186ab443 |
| Source note | uspto-grants-1995_01 |