HCID 67588708, compound → HCID 67588885, compound

Participants

Reaction Steps

4-(3',4',5'-Trifluorophenyl)ethoxycarbonylmethylenecyclohexane (18.3 g) was dissolved in ethanol (100 ml), followed by adding Pd/C (5%, 5 g), stirring the mixture, hydrogenating in a hydrogen gas atmosphere until completion of absorption of a hydrogen, filtering off the catalyst after completion of the reaction, and concentrating the solvent under reduced pressure, to obtain 4 -(3',4',5'-trifluorophenyl)ethoxycarbonylmethylcyclohexane (17.2 g).

Provenance & Evidence