HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86748406, compound → HCID 86748405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86748406 | HCID 86748406 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86748405 | HCID 86748405 | 92% |
Reaction Steps
Pd/C (5% ) (1 g) was added to a solution of 1,1-ethylenedioxy -(2'-(4"-(3'",4'",5'"-trifluorophenyl)cyclohexyl)-ethyl)-3-cyclohexene (6.7 g) in ethanol (200 ml), followed by carrying out catalytic reduction in a hydrogen gas atmosphere, filtering off the catalyst after completion of the reaction and distilling off the solvent from the organic layer under reduced pressure, to obtain 1,1 -ethylenedioxy-(2'-(4"-(3'",4'",5'"-trifluorophenyl)cyclohexyl)ethyl)cyclohexane (6.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05382379 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-6add5a1461c44a099eb7e1f9f6af1e88 |
| Source note | uspto-grants-1995_01 |