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HRID1769621

反应详情

EQUATION

反应方程式

HRID 1769621 的结构方程式

REACTANTS

反应物

2
结构：c1ccc(N2CCNCC2)cc1
HCID7096

Phenylpiperazine

C10H14N2

结构：C=C(C(=O)O)c1ccccc1
HCID68114

Benzeneacetic acid, .alpha.-methylene-

C9H8O2

PRODUCTS

生成物

1
结构：O=C(O)C(CN1CCN(c2ccccc2)CC1)c1ccccc1
HCID19433570

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

1-Phenylpiperazine and atropic acid in ethanol is heated under reflux for 18 h, cooled to room temperature, and evaporated in vacuo. The solid is triturated with acetone to give the title product.

WORKUP

后处理

  1. temperatureunder reflux for 18 h
  2. customevaporated in vacuo
  3. customThe solid is triturated with acetone