HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Tolyl isocyanate → HCID 14996845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Tolyl isocyanate | HCID 69303 | — |
| Reactant | HCID 14996844 | HCID 14996844 | — |
| Product | HCID 14996845 | HCID 14996845 | 30.9% |
Reaction Steps
The procedure is analogous to that described in Example 1 but 0.9 g of 2-(2-amino-N-phenyl-acetamido)-N-methyl-N-phenylacetamide and 0.4 g of 3-methylphenyl isocyanate are used as the starting material. After recrystallization from a mixture of diethyl ether and ethyl acetate (60-40 by volume), 0.4 g of N-methyl-N-phenyl-2-{2-[3-(3-methylphenyl)ureido]-N-phenyl-acetamido}acetamide melting at 168° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05382590 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-b938d3d7b96b4f6984bd9da5e50fb66a |
| Source note | uspto-grants-1995_01 |