Propyl chloroformate → HCID 10270365, compound

Participants

Reaction Steps

A suspension of 15.5 g (50 mmol) 2-amino-5-(3,5-dichlorobenzylamino)-nitrobenzene is hydrogenated in a manner analogous with Example 1 (variant A) and worked up appropriately with 6.2 g (51 mmol) propyl chloroformate. 10.8 g of the end product are obtained in the form of the dihydrochloride. This forms colorless to pale pink crystals.

Provenance & Evidence