HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 2-(7-Methoxynaphthalen-1-yl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 2-(7-Methoxynaphthalen-1-yl)acetyl chloride | HCID 19385766 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-(7-Methoxynaphthalen-1-yl)acetamide | HCID 15149127 | — |
Reaction Steps
The (7-methoxynaphth-1-yl)acetyl chloride obtained above is dissolved in 200 cm3 of anhydrous ether. After cooling the solution with the aid of an ice-salt bath, 200 cm3 of an aqueous concentrated ammonia solution are added, with stirring. The mixture is stirred for 30 minutes, and the resulting precipitate is suction filtered. The product is recrystallised in ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05385944 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-960ed8bd9d964c99865740ac5ff6b9c6 |
| Source note | uspto-grants-1995_01 |