1-Hexene → HCID 20096049, compound

Participants

Reaction Steps

In the same apparatus and procedures as EXAMPLE 1, 12.7 g (0.049 mole) of 3-(2,5-dimethylphenyl)-1,1-dimethoxy-1-silabutane, 13.1 g (0.15 mole) of 1-hexene, and 90 μl of 1% chloroplatinic acid in isopropanol were placed under the dry nitrogen atmosphere. The reactor was refluxed for 3 hours. Vacuum distillation of the reaction products gave 9.4 g (bp, 131°-3° C./0.6 mmHg) of 4,4-dimethoxy-2-(2,5-dimethylphenyl)-4-siladecane.

Provenance & Evidence