Salicylaldehyde → HCID 12155969, compound

HRID 1770514Notes

Reaction equation

HRID 1770514 reaction equation
[CH3:1][O:2][C:3](=[O:6])[CH2:4][NH2:5].[OH:7][C:8]1[CH:15]=[CH:14][CH:13]=[CH:12][C:9]=1[CH:10]=O>>[OH:7][C:8]1[CH:15]=[CH:14][CH:13]=[CH:12][C:9]=1[CH2:10][NH:5][CH2:4][C:3]([O:2][CH3:1])=[O:6]

Participants

3

Reactant 2

HCID 6998SalicylaldehydeHCID 69221Glycine methyl ester

Product 1

HCID 12155969HCID 12155969, compoundYield 40%

Procedure

Prepared as in example 10-10a from glycine methyl ester and 2-hydroxybenzaldehyde. Yield 40%. MS M+H calculated 196.1. Found 196.1

Sources & evidence

ORD record
ord-f4e9bead6fa3407ab08eb13b25a6e5cc
Source dataset
uspto-grants-2016_02
Patent number
US09247759B2

Reaction notes

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