HCID 67507979, compound → HCID 86665512, compound

Participants

Reaction Steps

A solution of benzyl 4-(2-hydroxyethylsulfonyl)-2-methylbutan-2-ylcarbamate (790 mg, 2.40 mmol) in methanol (30 ml) was purged with nitrogen and palladium on carbon (10%, 120 mg) was added. The solution was put under a blanket of hydrogen (1.3 atmospheres) and stirred for 1.5 hours at room temperature. The suspension was filtered through 0.45 um PTFE and concentrated in vacuo to afford the title compound which was used without further purification. LRMS (ESI/APCI) m/z 196 [M+H]+.

Provenance & Evidence