HCID 69093566, compound → HCID 86665517, compound

Participants

Reaction Steps

To a solution of 3-(3-(benzyloxycarbonylamino)-3-methylbutylsulfonyl)propane-1,2-diyl diacetate (401.9 mg, 0.9062 mmol) in methanol (10 ml) was added palladium on carbon (10%, 45 mg). The solution was purged with nitrogen gas, and then the suspension was put under a blanket of hydrogen gas (1.3 atm). The suspension was stirred for 1.5 hours, filtered through a 0.45 um PTFE filter, and concentrated in vacuo. The residue was used without any further purification. LRMS (ESI/APCI) m/z 310 [M+H]+.

Provenance & Evidence