HCID 67517747, compound → HCID 86665533, compound

Participants

Reaction Steps

A solution of benzyl 4-(2-(2-(2-tert-butoxyethoxy)ethoxy)ethylsulfonyl)-2-methylbutan-2-ylcarbamate (79.5 mg, 0.168 mmol) in MeOH (2 ml) was put under a N2 atmosphere and 10% Pd/C (30 mg) was added. A H2 atmosphere (1.3 atm) was added, and the slurry stirred for 2 h. The suspension was filtered (0.45 um PTFE) and the solution concentrated in vacuo. The residue was used without further purification. LRMS (ESI/APCI): 340 [M+H]+.

Provenance & Evidence