HCID 67509654, compound → HCID 86665534, compound

Participants

Reaction Steps

A solution of benzyl 4-(2-(2-(2-ethoxyethoxy)ethoxy)ethylsulfonyl)-2-methylbutan-2-ylcarbamate (119.8 mg, 0.2691 mmol) in MeOH (3 ml) was put under N2 and 10% Pd/C (12.6 mg) was added. The vessel was pressurized with H2 (1.3 atm) and the suspension stirred vigorously for 1.5 h. The suspension was filtered through a PTFE (0.45 um) filter and concentrated in vacuo, and the residue used without any further purification. LRMS (ESI/APCI): 312 [M+H]+.

Provenance & Evidence