HCID 67508302, compound → HCID 86665536, compound

Participants

Reaction Steps

A solution of benzyl 2-methyl-4-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethylsulfonyl)butan-2-ylcarbamate (6.07 g, 12.8 mmol) was dissolved in methanol (150 ml) was purged with N2. 10% palladium on carbon (890 mg) was added, and the suspension was put under a H2 (1.3 atmospheres) atmosphere. The suspension was stirred for 5 hours, filtered through Celite, and the solution concentrated in vacuo. The material was used without further purification. LRMS (ESI/APCI): 342 [M+H]+.

Provenance & Evidence