HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → 2-Carboxyethyl 5-amino-4-oxopentanoate hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 2-(t-butoxycarbonyl)ethyl 5-(Boc-amino)-4-oxopentanoate | HCID 90034512 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2-Carboxyethyl 5-amino-4-oxopentanoate hydrobromide | HCID 90034481 | 79% |
Reaction Steps
This compound was prepared from the product of 4a (5.43 g; 15.1 mmol) and 30% HBr in acetic acid (15 mL) according to Example 1c. 3.38 g (79%) product was obtained (amber gum that did not solidify).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249086B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-aadb54df4689413ba507b93820dbae30 |
| Source note | uspto-grants-2016_02 |