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HRID1771031

反应详情

EQUATION

反应方程式

HRID 1771031 的结构方程式

REACTANTS

反应物

2
结构：Br
HCID260

Hydrogen Bromide

BrH

结构：CC(C)(C)OC(=O)CCOC(=O)CCC(=O)CNC(=O)OC(C)(C)C
HCID90034512

未命名化合物

PRODUCTS

生成物

1
结构：Br.NCC(=O)CCC(=O)OCCC(=O)O
HCID90034481

未命名化合物

收率 79%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

This compound was prepared from the product of 4a (5.43 g; 15.1 mmol) and 30% HBr in acetic acid (15 mL) according to Example 1c. 3.38 g (79%) product was obtained (amber gum that did not solidify).