HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89474285, compound → HCID 89462331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89474285 | HCID 89474285 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 89462331 | HCID 89462331 | — |
Reaction Steps
A solution of tert-butyl (2,4-difluoro-3-(quinoxaline-6-carbonyl)phenyl)carbamate (600 mg, 1.56 mmol, 1 eq.) in HO/MeOH (6 N, 50 mL) was stirred at rt for 3 h, then concentrated to provide crude (3-amino-2,6-difluorophenyl) (quinoxalin-6-yl)methanone which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249110B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-77baba7c865a4f68837d3ec031a4a942 |
| Source note | uspto-grants-2016_02 |