反应详情

温度

25 °C

THF was added to a mixture of Salen and Et2Zn via a syringe under argon. The reaction mixture was stirred at 25° C. for 24 hours. The crude product was isolated from the concentrated reaction mixture by removal of the solvent under reduced pressure. A pure product Salen-Zn was obtained after recrystallization using THF and water.

1. customThe crude product was isolated from the concentrated reaction mixture by removal of the solvent under reduced pressure