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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1771260Generated: November 3, 2026

HCID 178418750, compound → HCID 178515947, compound

https://huagongshe.com/reaction/1771260

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178418750HCID 178418750—
ReactantHCID 178515945HCID 178515945—
SolventTetrahydrofuranHCID 8028—
ProductHCID 178515947HCID 178515947—

Reaction Conditions

Temperature25 °C

Reaction Steps

The Et2Zn (0.4 ml, 1.0 M in hexane) and Salen (N′N′-bis(3-tert-butyl-5-bromo-salicylidene)-1,2-diaminocyclohexane (0.4 mmol) and were dissolved in dried THF (20 ml). The mixture was stirred under argon at 25° C. for 24 hours. After that the compound Salen-Zn was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09249120B2
Source datasetuspto-grants-2016_02
ORD IDord-d5ca8491425f4909912a220ef84b675a
Source noteuspto-grants-2016_02