HuagongsheHuagongshe Chemistry Print Report · For research reference only
Selenium Dioxide → HCID 86676113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Selenium Dioxide | HCID 24007 | — |
| Reactant | 1-(3-Chloro-5-fluorophenyl)ethan-1-one | HCID 2757531 | — |
| Product | HCID 86676113 | HCID 86676113 | 84% |
Reaction Steps
(3-Chloro-5-fluorophenyl)(oxo)acetaldehyde (27 g, 84%) was prepared from 3-chloro-5-fluoro acetophenone (30.0 g, 174.4 mmol) and selenium dioxide (21.28 g, 191.8 mmol) according to the typical procedure used for Preparation 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249130B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-95c8f8c2708b43dc8835642f3911bbc5 |
| Source note | uspto-grants-2016_02 |