HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glyoxal, phenyl-, hydrate → 3-(Methylthio)-5-phenyl-1,2,4-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glyoxal, phenyl-, hydrate | HCID 12215922 | — |
| Reactant | Methyl hydrazinecarbimidothioate | HCID 178504051 | — |
| Product | 3-(Methylthio)-5-phenyl-1,2,4-triazine | HCID 98541 | 73.2% |
Reaction Steps
3-(Methylsulfanyl)-5-phenyl-1,2,4-triazine (2.93 g, 73%) was prepared from methyl hydrazinecarbimidothioate (2.07 g, 19.7 mmol) and phenylglyoxal monohydrate (2.89 g, 19.7 mmol) according to the general procedure of Preparation 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249130B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-1f4678adfd4845d08fa001dbeb60a397 |
| Source note | uspto-grants-2016_02 |