HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 5-Phenyl-1,2,4-triazin-3-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 3-(Methylsulfonyl)-5-phenyl-1,2,4-triazine | HCID 10988221 | — |
| Product | 5-Phenyl-1,2,4-triazin-3-amine | HCID 97081 | 73% |
Reaction Steps
5-Phenyl-1,2,4-triazin-3-amine (1.70 g, 73%) was prepared from 3-(methylsulfonyl)-5-phenyl-1,2,4-triazine (3.20 g, 13.6 mmol) and 0.5 M ammonia in THF (100 mL, 500 mmol) according to the general procedure of Preparation 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249130B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-6c786a2bdeae4ca6b0c89652b82d21b9 |
| Source note | uspto-grants-2016_02 |