HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 89852317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | HCID 89851657 | HCID 89851657 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 89852317 | HCID 89852317 | 97% |
Reaction Steps
A mixture of methyl 2-((2-bromophenethyl)thio)acetate (4.4 g), 1-chloropyrrolidine-2,5-dione (2 g) and carbon tetrachloride (2.4 g) was stirred on ice-bath for 2.5 hrs, filtrated and evaporated to yield the title compound (4.7 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249127B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-6fb8eb04fc6b4f6483849ea83d3b7f7e |
| Source note | uspto-grants-2016_02 |