Chlorosuccinimide → HCID 89852317, compound

HRID 1771426Notes

Reaction equation

HRID 1771426 reaction equation
[Br:1][C:2]1[CH:15]=[CH:14][CH:13]=[CH:12][C:3]=1[CH2:4][CH2:5][S:6][CH2:7][C:8]([O:10][CH3:11])=[O:9].[Cl:16]N1C(=O)CCC1=O>C(Cl)(Cl)(Cl)Cl>[CH3:11][O:10][C:8](=[O:9])[CH:7]([S:6][CH2:5][CH2:4][C:3]1[CH:12]=[CH:13][CH:14]=[CH:15][C:2]=1[Br:1])[Cl:16]

Participants

4

Reactant 2

HCID 31398ChlorosuccinimideHCID 89851657HCID 89851657, compound

Product 1

HCID 89852317HCID 89852317, compoundYield 97%

Reagents, catalysts & solvents 1

HCID 5943Carbon TetrachlorideSolvent

Procedure

A mixture of methyl 2-((2-bromophenethyl)thio)acetate (4.4 g), 1-chloropyrrolidine-2,5-dione (2 g) and carbon tetrachloride (2.4 g) was stirred on ice-bath for 2.5 hrs, filtrated and evaporated to yield the title compound (4.7 g).

Workup

  1. filtrationfiltrated
  2. customevaporated

Sources & evidence

ORD record
ord-6fb8eb04fc6b4f6483849ea83d3b7f7e
Source dataset
uspto-grants-2016_02
Patent number
US09249127B2

Reaction notes

Loading…