反应详情

A mixture of methyl 2-((2-bromophenethyl)thio)-2-chloroacetate (4.7 g), aluminum trichloride (2 g) and DCM (15 ml) was stirred in ice bath and allowed to warm up to ambient temperature and stirred 3.5 hrs. Separation method B and E yielded the title compound (2.9 g).

1. stirringstirred 3.5 hrs
2. customSeparation method B and E