HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminum(III) Chloride → HCID 89852398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 89852317 | HCID 89852317 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 89852398 | HCID 89852398 | 69.5% |
Reaction Steps
A mixture of methyl 2-((2-bromophenethyl)thio)-2-chloroacetate (4.7 g), aluminum trichloride (2 g) and DCM (15 ml) was stirred in ice bath and allowed to warm up to ambient temperature and stirred 3.5 hrs. Separation method B and E yielded the title compound (2.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249127B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-f8fff554b22547bda12cfadc2fa35fcd |
| Source note | uspto-grants-2016_02 |