HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 71767645, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 71767501 | HCID 71767501 | — |
| Product | HCID 71767645 | HCID 71767645 | — |
Reaction Steps
2-(7-Methoxy-5-methylisochroman-1-yl)-4,5-dihydro-1H-imidazole (example 61, 100 mg) was dissolved in hydrobromic acid (1.5 mL, 47 w-% in water) and mixture was heated to reflux. After 5.5 hours mixture was cooled down to room temperature. Solvents were evaporated and the evaporation residue was triturated with ethanol to afford the title compound. (Yield 27 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249127B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-0265cf1f738140aa83c2d17745cc1d5e |
| Source note | uspto-grants-2016_02 |