HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89851907, compound → HCID 89851705, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89851907 | HCID 89851907 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 89851705 | HCID 89851705 | — |
Reaction Steps
To a solution of 1-(2-(benzyloxy)-4-fluorobutyl)-2-methylbenzene (3.0 g, 11.03 mmol) in MeOH (50 ml) was added 10% Pd/C (0.3 g) under nitrogen and stirred at 40 psi for 5 h. The reaction mixture was filtered through Celite and concentrated under reduced pressure to afford crude compound. The title compound was purified by separation method E. (Yield 1.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249127B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-7ef99682770f4d539486b971400579c3 |
| Source note | uspto-grants-2016_02 |