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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1771442Generated: November 4, 2026

HCID 89851907, compound → HCID 89851705, compound

https://huagongshe.com/reaction/1771442

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 89851907HCID 89851907—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 89851705HCID 89851705—

Reaction Steps

To a solution of 1-(2-(benzyloxy)-4-fluorobutyl)-2-methylbenzene (3.0 g, 11.03 mmol) in MeOH (50 ml) was added 10% Pd/C (0.3 g) under nitrogen and stirred at 40 psi for 5 h. The reaction mixture was filtered through Celite and concentrated under reduced pressure to afford crude compound. The title compound was purified by separation method E. (Yield 1.5 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09249127B2
Source datasetuspto-grants-2016_02
ORD IDord-7ef99682770f4d539486b971400579c3
Source noteuspto-grants-2016_02