HuagongsheHuagongshe Chemistry Print Report · For research reference only
(6-Hydroxynaphthalen-2-yl)boronic acid → HCID 136069515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (6-Hydroxynaphthalen-2-yl)boronic acid | HCID 4349738 | — |
| Reactant | Methyl 6-chloropyridazine-3-carboxylate | HCID 12379801 | — |
| Product | HCID 136069515 | HCID 136069515 | — |
Reaction Steps
Followed the two step procedure described for Example 7 starting from 6-hydroxynaphthalen-2-ylboronic acid and methyl 6-chloropyridazine-3-carboxylate. 1H-NMR (DMSO-d6 500 MHz): 10.16 (s, 1H), 8.71 (d, J=5.0 Hz, 1H), 8.51-8.48 (m, 1H), 8.30-8.23 (m, 2H), 7.97-7.86 (m, 2H), 7.23-7.19 (m, 2H). MS (ESI): m/z 267.0 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249132B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-fe0770c10b8a476abc84b21c604f59ff |
| Source note | uspto-grants-2016_02 |