HuagongsheHuagongshe Chemistry Print Report · For research reference only
(6-Hydroxynaphthalen-2-yl)boronic acid → HCID 57386908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (6-Hydroxynaphthalen-2-yl)boronic acid | HCID 4349738 | — |
| Reactant | Methyl 5-bromopyrimidine-2-carboxylate | HCID 45790831 | — |
| Product | HCID 57386908 | HCID 57386908 | — |
Reaction Steps
Followed the two step procedure described for Example 7 starting from 6-hydroxynaphthalen-2-yl boronic acid and methyl 5-bromopyrimidine-2-carboxylate. 1H-NMR (DMSO-d6 500 MHz): 9.39 (s, 2H), 8.38 (s, 1H), 7.87-7.91 (t, J=8.5, 12.0 Hz, 3H), 7.17-7.20 (t, J=5.5, 10.5 Hz, 2H). MS (ESI): m/z=267.0 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249132B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-f29cc054e385492d98cc6b578c5c041c |
| Source note | uspto-grants-2016_02 |