HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → HCID 53380041, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | HCID 68233577 | HCID 68233577 | — |
| Product | HCID 53380041 | HCID 53380041 | — |
Reaction Steps
Method as for example 58 using (S)-phenyl(4-(4-(5-fluoro-2-(methylsulfonyl)phenyl)-6-(3-methylmorpholino)pyrimidin-2-yl)phenyl)carbamate (intermediate 34) and cyclopropyl amine as starting materials. The solvent removed in vacuo and the crude material purified by prep HPLC at low pH to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249129B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-0eb7c57d06df4c79be2f75f42eb45475 |
| Source note | uspto-grants-2016_02 |