HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-3-methylpyridine → HCID 178425976, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-3-methylpyridine | HCID 15347 | — |
| Reactant | O-(2,4,6-Trimethylbenzenesulfonyl)hydroxylamine | HCID 11830845 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178425976 | HCID 178425976 | — |
Reaction Steps
A solution of O-(mesitylsulfonyl)hydroxylamine (6.45 g, 30.0 mmol) in DCM (30 mL) was stirred at room temperature, then 2-amino-3-methylpyridine (1.08 g, 10.0 mmol) was added slowly. The reaction mixture was stirred at room temperature for 12 h, the solvent was removed under vacuum, and the crude product was used for the next step without further purification. ESI MS: m/z 124 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249162B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-014fc706645f40d2832b6bcf853743bc |
| Source note | uspto-grants-2016_02 |