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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1772305Generated: November 1, 2026

Trimethylsilyl iodide → HCID 67501441, compound

https://huagongshe.com/reaction/1772305

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrimethylsilyl iodideHCID 85247—
ReactantHCID 11395197HCID 11395197—
ReactantHCID 66781128HCID 66781128—
ProductHCID 67501441HCID 6750144173%

Reaction Steps

This compound was prepared as described for 3f, using 22 (200 mg, 0.53 mmol) as a starting material and iodotrimethysilane (0.6 mL, 4.2 mmol). Compound 3h (130 mg, 0.38 mmol) was obtained as a colorless solid, in 73% yield, which was characterized as follows:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09249177B2
Source datasetuspto-grants-2016_02
ORD IDord-5220f0fab1b64a7a975f07df73e9d499
Source noteuspto-grants-2016_02