HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloromethyl 2-(trimethylsilyl)ethyl ether → HCID 123860259, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloromethyl 2-(trimethylsilyl)ethyl ether | HCID 2724271 | — |
| Reactant | 1-(4-Bromophenyl)-1,2-dihydro-3H-1,2,4-triazol-3-one | HCID 23434192 | — |
| Product | HCID 123860259 | HCID 123860259 | 58% |
Reaction Steps
Compound 11b (30.0 g, 125 mmol) was treated with SEMCl using the reaction conditions described in Example 10, Step C to obtain compound 11c as a white solid (30.0 g, 58% yield). Mass Spectrum (LCMS, ESI pos.): Calcd. for C14H20BrN3O2S: 370.1 (M+H). Found 370.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249163B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-e79b0d5e55314533a78afe896f6d062d |
| Source note | uspto-grants-2016_02 |