2-Nitrobenzenesulfonyl chloride → HCID 26970545, compound

HRID 1772855Notes

Reaction equation

HRID 1772855 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[S:10](Cl)(=[O:12])=[O:11])([O-:3])=[O:2].[NH2:14][C:15]1[CH:16]=[CH:17][C:18]([O:21][CH3:22])=[N:19][CH:20]=1>>[CH3:22][O:21][C:18]1[N:19]=[CH:20][C:15]([NH:14][S:10]([C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N+:1]([O-:3])=[O:2])(=[O:12])=[O:11])=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 155402-Nitrobenzenesulfonyl chlorideHCID 811216-Methoxy-3-pyridinylamine

Product 1

HCID 26970545HCID 26970545, compoundYield 68%

Procedure

The title compound (1.05 g, 3.4 mmol) was prepared from 2-nitrobenzenesulfonyl chloride (1.1 g, 5.0 mmol) and 5-amino-2-methoxypyridine (683 mg, 5.5 mmol) using the methods of (IntA1), step 1.

Sources & evidence

ORD record
ord-f9fb55ce095b4766bde8edc2dcfcfa3a
Source dataset
uspto-grants-2016_02
Patent number
US09249160B2

Reaction notes

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