HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphosgene → HCID 90055161, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphosgene | HCID 94429 | — |
| Reactant | HCID 90030819 | HCID 90030819 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 90055161 | HCID 90055161 | 26.4% |
Reaction Steps
The title compound (0.20 g, 0.63 mmol) was prepared from 2-amino-N-[6-(dimethylamino)pyridin-2-yl]benzenesulfonamide (0.7 g, 2.39 mmol) and triphosgene (2.5 g, 8.3 mmol) in 1,4-dioxane (25 mL) using the methods of (IntA1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249160B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-58ac883ab4e84a2f8e08a8ec862cef32 |
| Source note | uspto-grants-2016_02 |