HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → N-(5,6-Dimethoxypyridin-3-yl)-2-nitrobenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2-Nitrobenzenesulfonyl chloride | HCID 15540 | — |
| Reactant | 5,6-Dimethoxypyridin-3-amine | HCID 12758214 | — |
| Product | N-(5,6-Dimethoxypyridin-3-yl)-2-nitrobenzenesulfonamide | HCID 118045902 | 38.3% |
Reaction Steps
The title compound (1.56 g, 4.60 mmol) was prepared from 2-nitrobenzenesulfonyl chloride (2.66 g, 12.0 mmol), 5,6-dimethoxy-3-pyridinamine (2.04 g, 13.2 mmol) and pyridine (2.9 mL, 36.0 mmol) using the methods of (IntA1), step 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249160B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-d157be4b095141daaeb6de0947898412 |
| Source note | uspto-grants-2016_02 |