HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethylaniline → HCID 43388285, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethylaniline | HCID 7949 | — |
| Reactant | 2-Chloropyridine-3-sulfonyl chloride | HCID 10219968 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 43388285 | HCID 43388285 | 52.1% |
Reaction Steps
The title compound (791 mg, 2.67 mmol) was prepared from 2-chloropyridine-3-sulfonyl chloride (1.09 g, 5.12 mmol) and 3,5-dimethylaniline (709 uL, 5.65 mmol) in 1,4-dioxane (30 mL) using the methods of (IntC1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249160B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-8fdd2ac802e74c1fad18a8b8de6fc8b9 |
| Source note | uspto-grants-2016_02 |