HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Aminobenzothiazole → N-(1,3-Benzothiazol-6-yl)-2-chloropyridine-3-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Aminobenzothiazole | HCID 68288 | — |
| Reactant | 2-Chloropyridine-3-sulfonyl chloride | HCID 10219968 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | N-(1,3-Benzothiazol-6-yl)-2-chloropyridine-3-sulfonamide | HCID 90030239 | 50.8% |
Reaction Steps
The title compound (1.1 g, 3.38 mmol) was prepared from 2-chloropyridine-3-sulfonyl chloride (1.56 g, 7.36 mmol), 1,3-benzothiazol-6-amine (1.0 g, 6.66 mmol) and pyridine (10 mL) at rt using the methods of (IntC1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249160B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-f04a18d6559a4884b5636e6589fe8780 |
| Source note | uspto-grants-2016_02 |