Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6-Amino-2,3-dimethylpyridine → 2-chloro-N-(5,6-dimethylpyridin-2-yl)pyridine-3-sulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6-Amino-2,3-dimethylpyridine | HCID 262484 | — |
| 반응물 | 2-Chloropyridine-3-sulfonyl chloride | HCID 10219968 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 2-chloro-N-(5,6-dimethylpyridin-2-yl)pyridine-3-sulfonamide | HCID 90030679 | 85.7% |
반응 단계
The title compound (5.0 g, 16.8 mmol) was prepared from 2-chloropyridine-3-sulfonyl chloride (5.0 g, 23.7 mmol) and 5,6-dimethylpyridin-2-amine (2.4 g, 19.6 mmol) in pyridine (25 mL) at rt using the methods of (IntC1), step 1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09249160B2 |
| 출처 데이터셋 | uspto-grants-2016_02 |
| ORD ID | ord-fbb73121577d4a2b909a4d4609d65a3d |
| 출처 메모 | uspto-grants-2016_02 |